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Volume 3 Issue 1
Nov.  2020
Article Contents

Dobbelstein H, George E P, Gurevich E L, Kostka A, Ostendorf A, Laplanche G. 2021. Laser metal deposition of refractory high-entropy alloys for high-throughput synthesis and structure-property characterization. Int. J. Extrem. Manuf. 3, 015201.
Citation: Dobbelstein H, George E P, Gurevich E L, Kostka A, Ostendorf A, Laplanche G. 2021. Laser metal deposition of refractory high-entropy alloys for high-throughput synthesis and structure-property characterization. Int. J. Extrem. Manuf. 3, 015201.

Laser metal deposition of refractory high-entropy alloys for high-throughput synthesis and structure-property characterization


doi: 10.1088/2631-7990/abcca8
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  • Publish Date: 2020-11-13
  • Progress in materials development is often paced by the time required to produce and evaluate a large number of alloys with different chemical compositions. This applies especially to refractory high-entropy alloys (RHEAs), which are difficult to synthesize and process by conventional methods. To evaluate a possible way to accelerate the process, high-throughput laser metal deposition was used in this work to prepare a quinary RHEA, TiZrNbHfTa, as well as its quaternary and ternary subsystems by in-situ alloying of elemental powders. Compositionally graded variants of the quinary RHEA were also analyzed. Our results show that the influence of various parameters such as powder shape and purity, alloy composition, and especially the solidification range, on the processability, microstructure, porosity, and mechanical properties can be investigated rapidly. The strength of these alloys was mainly affected by the oxygen and nitrogen contents of the starting powders, while substitutional solid solution strengthening played a minor role.

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Laser metal deposition of refractory high-entropy alloys for high-throughput synthesis and structure-property characterization

doi: 10.1088/2631-7990/abcca8
  • 1 Applied Laser Technologies, Ruhr-University Bochum, Universitätsstr. 150, 44801 Bochum, Germany
  • 2 Material Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831-6115, United States of America
  • 3 Materials Science and Engineering Department, University of Tennessee, Knoxville, TN 37996-2100, United States of America
  • 4 Center for Interface-Dominated High Performance Materials, Ruhr-University Bochum, Universitätsstr. 150, 44801 Bochum, Germany
  • 5 Institute for Materials, Ruhr-University Bochum, Universitätsstr. 150, 44801 Bochum, Germany

Abstract: 

Progress in materials development is often paced by the time required to produce and evaluate a large number of alloys with different chemical compositions. This applies especially to refractory high-entropy alloys (RHEAs), which are difficult to synthesize and process by conventional methods. To evaluate a possible way to accelerate the process, high-throughput laser metal deposition was used in this work to prepare a quinary RHEA, TiZrNbHfTa, as well as its quaternary and ternary subsystems by in-situ alloying of elemental powders. Compositionally graded variants of the quinary RHEA were also analyzed. Our results show that the influence of various parameters such as powder shape and purity, alloy composition, and especially the solidification range, on the processability, microstructure, porosity, and mechanical properties can be investigated rapidly. The strength of these alloys was mainly affected by the oxygen and nitrogen contents of the starting powders, while substitutional solid solution strengthening played a minor role.

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